Setsi sa concentrator ea ho ntša litlama

Kopo

Yuniti ena ke yuniti e kopantsoeng ea ho hula le mahloriso, e ka sebelisoang liunivesithing, litsi tsa lipatlisiso tsa mahlale, lipetlele, likhoebo, joalo-joalo joalo ka boikemisetso ba litekanyetso tse ncha tsa thekenoloji ea tlhahiso ea lithethefatsi, liteko tsa lipakeng, nts'etsopele ea mefuta e mecha, ho ntšoa ha thepa ea bohlokoa ea meriana, ho fetoha ha maemo. ho hlaphoheloa ha oli, joalo-joalo Sehlopha se na le mesebetsi e feletseng, e ka finyellang litlhoko tsa ho ntšoa ha oli e sa tsitsang, ho ntšoa ha metsi, ho ntšoa ha joala, ho ntšoa ha metsi le ho chesoa ha reflux e chesang, 'me e ka tsosolosa solvent ea manyolo.Matla a khoheli a khethehileng a motsoako o tsitsitseng a ka qetella a fihla ho 1.3, 'me lerako le ka hare la concentrator ha le phehiloe' me ho tsoa ho boreleli.Likarolo ka kakaretso li na le lisebelisoa tse lekaneng, li kopane, li nyane ebile li ntle ka chebahalo, li bonolo ho sebetsa le ho li hlokomela, 'me li fihlela litlhoko tsa tšebeliso tlasa maemo a laboratori.Ho kenyeletsoa tanka e ntšang mesebetsi e mengata, sekontiri se silafatsang sekontiri, pompo e thibelang ho phatloha ha metsi a sepakapaka le sistimi e futhumatsang oli e phahameng, hammoho le liphaephe tsohle le li-valve.

Sebopeho sa setsi sa concentrator se ntšang litlama

1.Thepa ena e na le tlhahiso e ntle haholo, collocation e felletseng, ts'ebetso e bonolo.E na le tanka ea ho ntša, pitsa e tebileng, tanka ea polokelo bakeng sa ho nchafatsa lintho tse nang le metsi, condenser, karohano ea metsi a oli, filthara, pompo ea phano, pompo ea vacuum joalo-joalo.Re na le ho futhumatsa mouoane le ho futhumatsa motlakase, mosebelisi a ka o sebelisa feela ho kenya mouoane kapa motlakase.
2.Thepa ena e bokella ho ntšoa, mahloriso a vacuum, ho hlaphoheloa ha solvent hammoho 'me e khona ho lemoha ts'ebetso ea mocheso o tloaelehileng oa mocheso, mocheso o tlaase oa mocheso, mocheso o chesang, mocheso o tlaase oa mocheso, mocheso o tlaase le pokello ea oli ea bohlokoa joalo-joalo. ho 1.4 mme mocheso o ka laoloa ka bolokolohi pakeng tsa 48-100 ° C, kahoo o loketse ka ho khetheha bakeng sa lisebelisoa tse ling tse phahameng tsa mocheso 'me lisebelisoa tse ling li na le mocheso o phahameng.
3.Thepa ena e ka lokisa le tsamaiso ea taolo ea PLC ho ea ka tlhokahalo ea mosebedisi le ho laola parameter nakong ea ts'ebetso ho ntlafatsa katleho ea tlhahiso le boleng.

Molemo

1) Eketsa solvent hang bakeng sa bohle, 'me tšebeliso e theoleloa ho feta 40%.Ka reflux e chesang, ho potoloha ho qobelloa le ho ntša soxhlet ho kopantsoe, solute e boloka gradient e phahameng ka har'a solvent, e eketsa tekanyo ea ho amohela ka 10 ho ea ho 15%.

2) Ho hokela le ho sebelisa sekontiri hape ho etsa hore sesebelisoa se lumellane le ho etsa hore karolo ka 'ngoe e bapaloe ka botlalo.Ntle le ho eketsa matsete a sesebelisoa, Ka bobeli reflux le ho hlaphoheloa ha solvent li ka fihlelleha ka phello e ntle.

3) Theknoloji e ncha le lisebelisoa tse ncha li sebelisoa bakeng sa ts'ebetso e ntle ea yuniti.Libaka tsa yuniti e amanang le metsi a bongaka le li-solvents ka lisebelisoa, lisebelisoa le liphaephe, li entsoe ka tšepe e phahameng e sa hloekang.